湖北农业科学 ›› 2019, Vol. 58 ›› Issue (8): 126-128.doi: 10.14088/j.cnki.issn0439-8114.2019.08.029

• 检测分析 • 上一篇    下一篇

不同干燥方法对商陆总皂苷和皂苷甲含量的影响

谢其亮1, 陈重2, 潘岩2, 杨俊杰2   

  1. 1.河南羚锐制药股份有限公司,河南 信阳 464000;
    2.信阳农林学院信阳市中药资源开发工程技术研究中心/信阳市中药分析检测重点实验室,河南 信阳 464000
  • 收稿日期:2018-06-29 出版日期:2019-04-25 发布日期:2019-12-04
  • 通讯作者: 杨俊杰(1979-),男,河南南阳人,副教授,硕士,主要从事中药材产地加工及活性成分开发研究,(电子信箱)nanyangjj@xyafu.edu.cn
  • 作者简介:谢其亮(1970-),男,河南信阳人,工程师,主要从事中药制药研究,(电话)13939722266(电子信箱)915036515@qq.com
  • 基金资助:
    国家中医药行业专项(2015468002-2); 信阳市科技攻关项目(150089)

Different dry means on the contents of total saponins and esculentoside A of Phytolacca americana

XIE Qi-liang1, CHEN Zhong2, PAN Yan2, YANG Jun-jie2   

  1. 1.Henan Lingrui Pharmaceutical Co.,Ltd.,Xinyang 464000,Henan,China;
    2.Xinyang Engineering Research Center for the Exploitation of Chinese Medicine Resources/Xinyang Key Laboratory of Detection and Analysis of Chinese Medicine, Xinyang Agriculture and Forestry University,Xinyang 464000,Henan,China
  • Received:2018-06-29 Online:2019-04-25 Published:2019-12-04

摘要: 利用硫酸-香草醛比色法测定商陆(Phytolacca americana)总皂苷含量,采用HPLC-UV法测定商陆皂苷甲的含量。结果表明,商陆总皂苷和皂苷甲的含量比较,阴干商陆明显低于其他组,晒干商陆次之,烘干品含量较高;其中低温55 ℃烘干品的商陆总皂苷含量最高,80 ℃烘干的商陆皂苷甲含量高于其他组。商陆产地加工中,应及时干燥,避免成分流失,规模化烘干优于传统晒干,采用低温烘干为宜。

关键词: 商陆(Phytolacca americana), 产地加工, 干燥方法, 总皂苷, 皂苷甲

Abstract: UV spectrophotometry was used to determine total saponins of Phytolacca americana by the sulphuric acid vanillin colorimetric method,HPLC-UV Method was used to determine the content of esculentoside A. Results showed that their contents of the group dry in the shade were Significantly lower than the other groups,the group dry in the sun were the second from the bottom,the group dry hot air were higher. Among them, the content of total saponin of Phytolacca americana was the highest dry at 55 ℃, and the content of esculentoside A was the highest dry at 80 ℃. It should be dried in time, avoiding the loss of ingredients, drying in large scale is better than traditional drying, and drying at low temperature is advisable.

Key words: Phytolacca americana, producing processing, drying method, total saponins, esculentoside A

中图分类号: