湖北农业科学 ›› 2023, Vol. 62 ›› Issue (4): 156-162.doi: 10.14088/j.cnki.issn0439-8114.2023.04.028

• 检测分析 • 上一篇    下一篇

基于12个产地的白及冻干片质量标准

徐雨生1,2, 滕晓梅1, 辛文锋3, 高明菊3, 田迎秋3, 余正勇3   

  1. 1.湖南农业大学农学院,长沙 410128;
    2.湖南杂交水稻研究中心杂交水稻国家重点实验室,长沙 410125;
    3.文山学院三七医药学院, 云南 文山 663000
  • 收稿日期:2021-11-30 出版日期:2023-04-25 发布日期:2023-05-12
  • 通讯作者: 余正勇(1992-),男,云南曲靖人,硕士,主要从事中药质量控制与产地加工研究,(电话)15912278983(电子信箱)yzy19921123@163.com。
  • 作者简介:徐雨生(1993-),男,安徽蚌埠人,在读博士研究生,研究方向为作物学,(电话)17608729717(电子信箱)18375349197@163.com。
  • 基金资助:
    国家自然科学基金项目(31900300); 云南省科技厅重大科技专项计划(2018F004)

Quality standards for Bletilla striata freeze-dried tablets based on 12 producing areas

XU Yu-sheng1,2, TENG Xiao-mei1, XIN Wen-feng3, GAO Ming-ju3, TIAN Ying-qiu3, YU Zheng-yong3   

  1. 1. College of Agronomy, Hunan Agricultural University, Changsha 410128, China;
    2. State key Laboratory of Hybrid Rice, Hunan Hybrid Rice Research Center, Changsha 410125, China;
    3. College of Notoginseng Medicine and Pharmacy, Wenshan University, Wenshan 663000, Yunnan, China
  • Received:2021-11-30 Online:2023-04-25 Published:2023-05-12

摘要: 基于12个产地的白及(Bletilla striata)药材,探究其冻干片的质量标准。通过鉴别不同产地白及冻干片的一般理化性质,测定总多糖含量、含水量、总灰分含量、二氧化硫残留量、双[4- (β-D-吡喃葡萄糖氧)苄基]-2-异丁基苹果酸酯(Militarine)含量、浸出物含量,对白及冻干片进行质量评价。结果表明,12个产地的白及冻干片总多糖含量为28.2%~50.9%,Militarine含量为5.32%~10.73%,白及冻干片中的总多糖含量、含水量、总灰分含量、浸出物含量和Militarine含量均符合《中华人民共和国药典:四部》(2015)标准。

关键词: 白及(Bletilla striata), 冻干片, 含量测定, 质量标准

Abstract: Based on the medicinal materials of Bletilla striata from 12 producing areas, the quality standards for its freeze-dried tablets were explored. By identifying the general physical and chemical properties of Bletilla striata freeze-dried tablets from different origins, and determining the total polysaccharide content, water content, total ash content, sulfur dioxide residue, the content of [4 -(β-D-glucopyranoxy) benzyl] -2-isobutyl malate Militarine and the content of extracts, the quality of Bletilla striata freeze-dried tablets was evaluated. The results showed that the total polysaccharide content of Bletilla striata freeze-dried tablets from 12 producing areas was 28.2%~50.9%, and the content of Militarine was 5.32%~10.73%. The total polysaccharide content, water content, total ash content, extract content, and Militarine content in Bletilla striata freeze-dried tablets complied with the standards of the “Pharmacopoeia of the People’s Republic of China: Four Parts”(2015 edition).

Key words: Bletilla striata, freeze-dried tablets, content determination, quality standard

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