不同净化方法对甘草有机氯农药残留测定的比较研究

doi:10.14088/j.cnki.issn0439-8114.2022.20.027

湖北农业科学 ›› 2022, Vol. 61 ›› Issue (20): 141-148.doi: 10.14088/j.cnki.issn0439-8114.2022.20.027

不同净化方法对甘草有机氯农药残留测定的比较研究

廖予菲, 王萍, 张瑞瑞, 程茜菲

陕西国际商贸学院医药学院,西安 712046

收稿日期:2021-09-14 出版日期:2022-10-25 发布日期:2022-11-23
作者简介:廖予菲（1985-）,女,陕西咸阳人,实验师,硕士,主要从事中药成分分析工作,（电话）18091043503（电子信箱）feifei198532@qq.com。
基金资助:
陕西省中医药管理局科研项目（2021-ZZ-ZY006）; 陕西省教育厅科研计划项目（21JK0520; 21JY002）

Comparative study on determination of organochlorine pesticide residues in Glycyrrhiza uralensis by different purification methods

LIAO Yu-fei, WANG Ping, ZHANG Rui-rui, CHENG Qian-fei

Faculty of Medicine, Shaanxi Institute of International Trade and Commerce, Xi'an 712046, China

Received:2021-09-14 Online:2022-10-25 Published:2022-11-23

摘要/Abstract

摘要： 以甘草（Glycyrrhiza uralensis）作为研究对象,采用气相色谱法,分别通过磺化法及QuEChERS法进行样品净化处理,对2种净化方法进行评价。结果表明,2种净化方法所制样品中杂质对9种有机氯测定均无干扰,相对而言,QuEChERS处理效果更佳,杂质较少。对比研究试验中,重复性、回收率、检测限测定结果均表明,QuEChERS法略优于磺化法。QuEChERS法操作简单,步骤少,能专属、快速、灵敏、准确地实现样品处理分析,可作为甘草样品农药残留量测定的净化方法。

关键词: 有机氯农药, 甘草（Glycyrrhiza uralensis）, 净化方法, QuEChERS法

Abstract: Taking Glycyrrhiza uralensis as the research object, gas chromatography was used to purify samples by the sulphonation method and QuEChERS method, and the two purification methods were evaluated. The results showed that the impurities in the samples prepared by the two purification methods had no interference to the determination of 9 organochlorines, the treatment effect of QuEChERS was better and the impurities were less. In the comparative study, the results of repeatability, recovery rate and detection limit showed that QuEChERS method was slightly better than the sulfonation method. QuEChERS method had the advantages of simple operation and few steps. It could be used as a purification method for the determination of pesticide residues in licorice samples, which was exclusive, rapid, sensitive and accurate.

Key words: organochlorine pesticides, Glycyrrhiza uralensis, purification method, QuEChERS method

中图分类号:

S481⁺.8

廖予菲, 王萍, 张瑞瑞, 程茜菲. 不同净化方法对甘草有机氯农药残留测定的比较研究[J]. 湖北农业科学, 2022, 61(20): 141-148.

LIAO Yu-fei, WANG Ping, ZHANG Rui-rui, CHENG Qian-fei. Comparative study on determination of organochlorine pesticide residues in Glycyrrhiza uralensis by different purification methods[J]. HUBEI AGRICULTURAL SCIENCES, 2022, 61(20): 141-148.

不同净化方法对甘草有机氯农药残留测定的比较研究

Comparative study on determination of organochlorine pesticide residues in Glycyrrhiza uralensis by different purification methods

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