湖北农业科学 ›› 2020, Vol. 59 ›› Issue (13): 137-139.doi: 10.14088/j.cnki.issn0439-8114.2020.13.031

• 检测分析 • 上一篇    下一篇

HS-SPME-GC-MS分析仙茅及酒仙茅的挥发性成分

王文通, 江汉美, 张智婧   

  1. 湖北中医药大学/湖北省药用植物研发中心,武汉 430065
  • 收稿日期:2020-04-26 出版日期:2020-07-10 发布日期:2020-09-03
  • 通讯作者: 江汉美,女,湖北武汉人,教授,主要从事中药质量控制与分析工作,(电话) 13807186811(电子信箱)13807186811@163.com。
  • 作者简介:王文通(1994-),男,吉林松原人,硕士,主要从事中药质量控制与分析工作,(电话)15926261905(电子信箱)751511146@qq.com。
  • 基金资助:
    湖北省技术创新专项重大项目(2016ACA146)

Analysis of volatile components in Curculigo orchioides and wine-processed by HS-SPME-GC-MS

WANG Wen-tong, JIANG Han-mei, ZHANG Zhi-jing   

  1. Hubei University of Chinese Medicine/ Research and Development Center of Medicinal Plant in Hubei Province, Wuhan 430065,China
  • Received:2020-04-26 Online:2020-07-10 Published:2020-09-03

摘要: 采用顶空固相微萃取法(HS-SPME)结合气质联用技术(GC-MS)对生仙茅(Curculigo orchioides Gaertn. )及酒仙茅的挥发性成分进行分析鉴定,并计算各成分相对百分含量。结果表明,生仙茅中分离出22个峰,鉴定出16种成分,占挥发性成分的72.73%,其中含量最高的为右旋萜二烯,占总挥发性成分的16.22%;从酒仙茅中分离出28个峰,鉴定出24种成分,占挥发性成分的85.71%,其中含量最高的为壬醛,占总挥发性成分的10.09%。仙茅酒制后部分挥发性成分消失,同时也增加了一些新的挥发性成分,为仙茅药材开发利用和临床运用提供科学依据。

关键词: 仙茅(Curculigo orchioides Gaertn. ), HS-SPME, GC-MS, 挥发性成分

Abstract: Headspace solid phase microextraction (HS-SPME) combined with gas chromatography-mass spectrometry (GC-MS) was used to analyze the volatile components of Curculigo orchioides and wine-processed, and the relative contents of each component were calculated. The results showed that 22 peaks were isolated from the volatile components of Curculigo orchioides, and 16 components were identified, accounting for 72.73% of the volatile components, of which the highest was dextroterpene, accounting for 16.22% of the total volatile components. 28 peaks were isolated from the volatile components of Curculigo orchioides, and 24 components were identified, accounting for 85.71% of the volatile components, the highest of which was nonanal, accounting for 10.09% of the total volatile components. Part of the volatile components disappeared and some new volatile components were added after the production of Curculigo orchioides. It can provide scientific basis for the development, utilization and clinical application of Curculigo orchioides.

Key words: Curculigo orchioides Gaertn., HS-SPME, GC-MS, volatile components

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